Abstract

At any point in the fabrication and installation of Grade 91 components, undesirable metallurgical conditions can develop as a result of incorrect heat treatment. Industry techniques for locating and evaluating these microstructures using nondestructive methods are necessary. Field hardness testing is commonly utilized to characterize Grade 91 steel installed in plants. However, it is apparent that there are numerous variables that can affect the results of field hardness testing. Thus, the results can vary significantly depending on the equipment and procedures used. The present study has been undertaken to identify the accuracy of hardness measurements made under controlled laboratory conditions. Measurements were performed on samples that had been subjected to a range of different tempering conditions. The trend in these data provides information relevant to understanding the metallurgical behavior of this steel. Comparison of the data also indicates how measurements made using different hardness testers and methods can be used to assess component condition.

References

1.
DiStefano
,
J. R.
and
Sikka
,
V. K.
, “
Summary of Modified 9Cr-1Mo Steel Development Program
,”
ORNL-6303
,
Oak Ridge National Laboratory
,
Oak Ridge, TN
,
1986
.
2.
King
,
J. F.
,
Sikka
,
V. K.
,
Santella
,
M. L.
,
Turner
,
J. F.
, and
Pickering
,
E. W.
, “
Weldability of Modified 9Cr-1Mo Steel
,”
ORNL-6299
,
Oak Ridge National Laboratory
,
Oak Ridge, TN
,
1986
.
3.
Brinkmann
,
C. R.
,
Sikka
,
V. K.
,
Horak
,
J. A.
, and
Santella
,
M. L.
, “
Long Term Creep Rupture Behavior of Modified 9Cr-1Mo Steel Base and Weldment Behavior
,”
ORNL/TM-10504
,
Oak Ridge National Laboratory
,
Oak Ridge, TN
,
1987
.
4.
ASTM E353-93
:
Standard Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys
,
Annual Book of ASTM Standards
,
ASTM International
,
West Conshohocken, PA
,
2006
.
5.
Holloman
,
J. H.
and
Jaffe
,
L. D.
, “
Time-Temperature Relations in Tempering Steel
,”
Trans. AIME
, Vol.
162
,
1945
, pp.
223
249
.
6.
ASTM E92-82
:
Standard Test Method for Vickers Hardness of Metallic Materials
,
Annual Book of ASTM Standards
,
ASTM International
,
West Conshohocken, PA
,
2003
.
7.
ASTM E384-11
:
Standard Test Method for Knoop and Vickers Hardness of Materials
,
Annual Book of ASTM Standards
,
ASTM International
,
West Conshohocken, PA
,
2011
.
8.
Siefert
,
J. A.
,
Shingledecker
,
J. P.
, and
Parker
,
J. D.
, “
Optimization of Vickers Hardness Parameters for Micro and Macro Indentation of Grade 91 Steel
,”
ASTM J. Test. Eval.
, Vol.
41
, No.
5
,
2013
.
9.
Electric Power Research Institute (EPRI)
,
Service Experience with Grade 91 Components
,
EPRI
,
Palo Alto, CA
,
2009
.
10.
Electric Power Research Institute (EPRI)
,
Guidelines and Specifications for High-Reliability Fossil Power Plants
,
EPRI
,
Palo Alto, CA
,
2011
.
11.
ASME
, “
Positive Material Identification Practice
,”
ASME Boiler and Pressure Vessel Code: An Internationally Recognized Code
,
American Society of Mechanical Engineers
,
New York
,
2011
.
12.
ASTM E140-07
:
Standard Hardness Conversion Tables for Metals Relationship among Brinell Hardness, Vickers Hardness, Rockwell Hardness, Superficial Hardness, Knoop Hardness, and Scleroscope Hardness
,
Annual Book of ASTM Standards
,
ASTM International
,
West Conshohocken, PA
,
2007
.
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